HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-6-chlorobenzaldehyde → 1-(2-Amino-6-chlorophenyl)ethan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-6-chlorobenzaldehyde | HCID 22399512 | — |
| Reactant | HCID 178418573 | HCID 178418573 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1-(2-Amino-6-chlorophenyl)ethan-1-ol | HCID 69315421 | — |
Reaction Steps
This compound was prepared using General Method 1 (EXAMPLE 1) from 2-amino-6-chlorobenzaldehyde (45 mg, 0.29 mmol) and methylmagnesium bromide (3 M in ether, 0.24 mL) to afford (±)-(2-amino-6-chlorophenyl)ethanol after flash chromatography (4:1 hexanes:ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442696B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-86eddd6d0ea64997b3a79bb7c1af894b |
| Source note | uspto-grants-2008_10 |