HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68703838, compound → HCID 68707842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68703838 | HCID 68703838 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68707842 | HCID 68707842 | — |
Reaction Steps
A mixture of 384 mg (0.83 mmol) of 4-chloro-N-[3-(3-methoxy-4-nitrobenzoyl)-2-methylindolizin-1-yl]benzamide and 115 mg of platinum oxide in 9 ml of dimethylformamide is stirred, under 5 bar of hydrogen, at room temperature for 24 hours, and then filtered on talc. The filtrate is concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442708B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-1ef58abd03d44fa89a0507f6471a7470 |
| Source note | uspto-grants-2008_10 |