HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6,7,8-Tetrahydro-1,3-dioxolo(4,5-g)isoquinoline → (7,8-Dihydro-5H-[1,3]dioxolo[4,5-g]isoquinolin-6-yl)-(2-isopropoxy-5-methanesulfonyl-phenyl)-methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6,7,8-Tetrahydro-1,3-dioxolo(4,5-g)isoquinoline | HCID 27013 | — |
| Reactant | 2-Isopropoxy-5-methylsulfonylbenzoic acid | HCID 21100237 | — |
| Product | (7,8-Dihydro-5H-[1,3]dioxolo[4,5-g]isoquinolin-6-yl)-(2-isopropoxy-5-methanesulfonyl-phenyl)-methanone | HCID 58677874 | — |
Reaction Steps
Prepared in analogy to example 1.1 from 5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline (CA [94143-83-6]) and 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example 2.1). MS (m/e): 418.4 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442710B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-84179ac5e20b4d4aa872ba91620afa85 |
| Source note | uspto-grants-2008_10 |