Trifluoroacetic acid → HCID 18376152, compound

Participants

Reaction Conditions

Reaction Steps

TFA. A solution of 5-(3-((2-benzylsulfanyl-ethyl)-(pyridine-3-sulfonyl)-amino)-propyl)-thiophene-2-carboxylic acid tert-butyl ester prepared of Example 3, Step B (0.038 g) in 1 mL CH2Cl2 was cooled to 0° C. and 1 mL TFA was added. The mixture was warmed to room temperature and was stirred for 1 h. The CH2Cl2 and TFA were removed by evaporation, azeotroping with added CH2Cl2 to yield the title compound (46.3 mg). MS 475 (M−1).

Provenance & Evidence