HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(1H-imidazol-1-yl)benzaldehyde → HCID 54139938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(1H-imidazol-1-yl)benzaldehyde | HCID 736530 | — |
| Reactant | Methyl 7-aminoheptanoate hydrochloride | HCID 13807349 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54139938 | HCID 54139938 | — |
Reaction Steps
The title compound of Step A was prepared from 7-amino-heptanoic acid methyl ester hydrochloride, of Preparation 1, and 4-imidazol-1-yl-benzaldehyde, of Preparation 43, using the method described in Example 1, Step A except that the mine was formed in MeOH with a reaction time of 1h. 1H NMR (400 MHz, CDCl3) δ 7.82 (m, 1H), 7.43 (d, 2H), 7.33 (d, 2H), 7.25 (m, 1H), 7.18 (m, 1H), 3.82 (s, 2H), 3.65 (s, 3H), 2.62 (t, 2H), 2.29 (t, 2H), 1.61 (m, 2H), 1.52 (m, 2H), 1.33 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442702B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-9eba4c931a0743cc98915695630a0762 |
| Source note | uspto-grants-2008_10 |