HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-4-(4-nitrophenyl)-1-piperazinepropanamine → HCID 69067851, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-4-(4-nitrophenyl)-1-piperazinepropanamine | HCID 69071744 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69067851 | HCID 69067851 | — |
Reaction Steps
A solution of 4-(4-(3-dimethylaminopropyl)piperazino)nitrobenzene (1.5 g) in methanol (50 mL) was hydrogenated at atmospheric pressure over Pd (5% on carbon) (0.3 g; 50% water content) for 4 h. The catalyst was filtered off and the solvent removed under reduced pressure to give the title compound as a brown solid
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442698B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-5a1a9c0b42284f04ab202ebd9add427b |
| Source note | uspto-grants-2008_10 |