HRID2117965
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 270 °C
PROCEDURE
实验过程
The p-nitrobenzoylpyrrolinone ester 11 (300 mg, 0.90 mmol) was irradiated with microwave radiation without solvent, heating to 270° C. for 15 minutes. The crude product was then allowed to cool, methanol was added and the solid filtered off and washed with methanol. This gave the furopyrrole 12 as a red solid (230 mg, 87%).
WORKUP
后处理
- temperatureto cool
- filtrationthe solid filtered off
- washwashed with methanol