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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2117965Generated: October 31, 2026

HCID 12192473, compound → HCID 178517440, compound

https://huagongshe.com/reaction/2117965

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 12192473HCID 12192473—
SolventMethanolHCID 887—
ProductHCID 178517440HCID 17851744087%

Reaction Conditions

Temperature270 °C

Reaction Steps

The p-nitrobenzoylpyrrolinone ester 11 (300 mg, 0.90 mmol) was irradiated with microwave radiation without solvent, heating to 270° C. for 15 minutes. The crude product was then allowed to cool, methanol was added and the solid filtered off and washed with methanol. This gave the furopyrrole 12 as a red solid (230 mg, 87%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07442804B2
Source datasetuspto-grants-2008_10
ORD IDord-4a7d6cde82674d339b117c4f59669fcc
Source noteuspto-grants-2008_10