HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 67151031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Reactant | HCID 67151152 | HCID 67151152 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 67151031 | HCID 67151031 | — |
Reaction Steps
A solution of 3-bromo-6-hydroxyphenanthrene-9,10-dione from Step 4 in acetone was treated with excess potassium carbonate, potassium iodide and (bromomethyl)cyclopropane. The mixture was heated at reflux overnight, followed by standard workup to yield 3-bromo-6-(cyclopropylmethoxy)phenanthrene-9,10-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442716B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-08a4f0dee9374c02b74d5c78c01fd0b9 |
| Source note | uspto-grants-2008_10 |