Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54119480 | HCID 54119480 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 55291491 | HCID 55291491 | — |
Reaction Steps
To a stirred solution of 5-amino-1-hydroxyindane (4.2 g, 0.26 mol) in methanol (100 mL) was added hydrochloric acid (100 mL, 1.0 N). The mixture was stirred at 40° C. for 2 h, and then was concentrated to dryness under vacuum to the product as gray powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07442808B2 |
|---|
| Source dataset | uspto-grants-2008_10 |
|---|
| ORD ID | ord-deb776fc955844058e808508b0b05242 |
|---|
| Source note | uspto-grants-2008_10 |
|---|
