Hydrochloric Acid → HCID 55291491, compound

HRID 2118105Notes

Reaction equation

HRID 2118105 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[CH:7](O)[CH2:6][CH2:5]2.Cl>CO>[CH2:5]1[C:4]2[C:8](=[CH:9][CH:10]=[C:2]([NH2:1])[CH:3]=2)[CH:7]=[CH:6]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 54119480HCID 54119480, compound

Product 1

HCID 55291491HCID 55291491, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Conditions

Temperature
40 °C

Procedure

To a stirred solution of 5-amino-1-hydroxyindane (4.2 g, 0.26 mol) in methanol (100 mL) was added hydrochloric acid (100 mL, 1.0 N). The mixture was stirred at 40° C. for 2 h, and then was concentrated to dryness under vacuum to the product as gray powder.

Workup

  1. concentrationwas concentrated to dryness under vacuum to the product as gray powder

Sources & evidence

ORD record
ord-deb776fc955844058e808508b0b05242
Source dataset
uspto-grants-2008_10
Patent number
US07442808B2

Reaction notes

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