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HRID2118130

反应详情

EQUATION

反应方程式

HRID 2118130 的结构方程式

REACTANTS

反应物

2
结构：BrC(c1ccccc1)c1ccccc1
HCID236603

Bromodiphenylmethane

C13H11Br

结构：CCOC(=O)c1[nH]c2ccc([N+](=O)[O-])cc2c1-c1ccccc1
HCID741309

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1c(-c2ccccc2)c2cc([N+](=O)[O-])ccc2n1C(c1ccccc1)c1ccccc1
HCID69228492

未命名化合物

PROCEDURE

实验过程

Ethyl 1-benzhydryl-5-nitro-3-phenyl-1H-indole-2-carboxylate was prepared from ethyl 5-nitro-3-phenyl-1H-indole-2-carboxylate and bromodiphenylmethane according to the procedure of Example 1 Step 1 as a yellowish solid: 1H NMR (CDCl3) δ 0.92 (t, J=7.1 Hz, 3H, 4.08 (q, J=7.1 Hz, 2H, 6.86 (d, J=9.4 Hz, 1H, 7.20-7.50 (m, 15H, 7.89 (dd, J=9.3, 2.3 Hz, 1H, 7.97 (s, 1H, 8.47 (d, J=2.3 Hz, 1H, MS (ESI) m/z 477 (MH+); HRMS calcd for C30H25N2O4: 477.1812; found (ESI+): 477.1808.