HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromodiphenylmethane → Ethyl 1-benzhydryl-5-nitro-3-phenyl-1H-indole-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromodiphenylmethane | HCID 236603 | — |
| Reactant | ethyl 5-nitro-3-phenyl-1H-indole-2-carboxylate | HCID 741309 | — |
| Product | Ethyl 1-benzhydryl-5-nitro-3-phenyl-1H-indole-2-carboxylate | HCID 69228492 | — |
Reaction Steps
Ethyl 1-benzhydryl-5-nitro-3-phenyl-1H-indole-2-carboxylate was prepared from ethyl 5-nitro-3-phenyl-1H-indole-2-carboxylate and bromodiphenylmethane according to the procedure of Example 1 Step 1 as a yellowish solid: 1H NMR (CDCl3) δ 0.92 (t, J=7.1 Hz, 3H, 4.08 (q, J=7.1 Hz, 2H, 6.86 (d, J=9.4 Hz, 1H, 7.20-7.50 (m, 15H, 7.89 (dd, J=9.3, 2.3 Hz, 1H, 7.97 (s, 1H, 8.47 (d, J=2.3 Hz, 1H, MS (ESI) m/z 477 (MH+); HRMS calcd for C30H25N2O4: 477.1812; found (ESI+): 477.1808.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442805B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-6c54e36043804bad82616a8f022e4285 |
| Source note | uspto-grants-2008_10 |