HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Sulfite → HCID 86609640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | 3-Iodobenzyl bromide | HCID 2759361 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86609640 | HCID 86609640 | 118.8% |
Reaction Steps
A solution of 3-iodobenzyl bromide (3 g) and sodium sulphite (1.26 g) in acetone (15 ml) and water (30 ml) was heated at 70° for 3 h. The solvent was removed under reduced pressure and the residue was triturated in ether to give the title compound (3.8 g). LCMS RT=3.66 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442836B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-613bc3abd211404c998dd2a8f31dc4a6 |
| Source note | uspto-grants-2008_10 |