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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2118354Generated: November 2, 2026

HCID 69119338, compound → HCID 69119693, compound

https://huagongshe.com/reaction/2118354

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69119338HCID 69119338—
SolventAcetic AcidHCID 176—
SolventWaterHCID 962—
ProductHCID 69119693HCID 69119693—

Reaction Steps

A solution of 2-[(6-{4-[3-(cyclopentylsulfonyl)phenyl]butoxy}hexyl)amino]-1-(2-phenyl-4H-[1,3]dioxino[5,4-b]pyridin-6-yl)ethanol (61 mg) in water (5 ml) and glacial acetic acid (5 ml) was heated under reflux for 0.5 h. The reaction mixture was concentrated in vacuo to afford the title compound. LCMS RT=2.63 min 548(M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07442839B2
Source datasetuspto-grants-2008_10
ORD IDord-b312788d4e224623850bbdce33cfcce3
Source noteuspto-grants-2008_10