HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-dichloro-N'-(pentafluorobenzoyl)benzohydrazide → HCID 21982111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-dichloro-N'-(pentafluorobenzoyl)benzohydrazide | HCID 21982129 | — |
| Solvent | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 21982111 | HCID 21982111 | 81% |
Reaction Steps
By the general method of Part B of Example 2, the reaction of 21.0 g (0.05377 mol) 2,5-dichloro-N′-(pentafluorobenzoyl)benzohydrazide in POCl3 gave a product which was recrystallized from ethanol/water to give 16.59 g (81% yield) of 2-(2,5-dichlorophenyl)-5-(pentafluorophenyl)-1,3,4-oxadiazole (10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442760B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-c9eac6709ceb479c844ebb4b93c58f0f |
| Source note | uspto-grants-2008_10 |