HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13923772, compound → HCID 20140561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13923772 | HCID 13923772 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20140561 | HCID 20140561 | 97.1% |
Reaction Steps
To a solution of 5.49 g (19.4 mmol) of material prepared in Example 11 in 250 mL of methylene chloride was added 8.35 g (39 mmol) of pyridiniumchlorochromate. After 3 hours the reaction mixture was diluted with ether and passed through a plug of fluorosil to give 5.3 g of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04678499 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-0562072ceb42464d99b6358580a9659c |
| Source note | uspto-grants-1987_07 |