2-Chlorobenzyl chloride → HCID 20194017, compound

HRID 2118508Notes

Reaction equation

HRID 2118508 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[N:8][CH2:7][CH2:6]2.[Cl:13][C:14]1[CH:21]=[CH:20][CH:19]=[CH:18][C:15]=1[CH2:16]Cl.O1CCOCC1>C(Cl)CCl>[Cl-:13].[Cl:13][C:14]1[CH:21]=[CH:20][CH:19]=[CH:18][C:15]=1[CH2:16][N+:8]1[CH2:7][CH2:6][C:5]2[C:10](=[CH:11][CH:12]=[C:3]([O:2][CH3:1])[CH:4]=2)[CH:9]=1

Participants

5

Reactant 3

HCID 119062-Chlorobenzyl chlorideHCID 312751,4-DioxaneHCID 1001219614446-29-8

Product 1

HCID 20194017HCID 20194017, compound

Reagents, catalysts & solvents 1

HCID 111,2-DichloroethaneSolvent

Procedure

The title compound is prepared analogously to Example A from 6-methoxy-3,4-dihydro-isoquinoline and 2-chlorobenzyl chloride in ethylene chloride. Melting point: 156°-158° C. (Decomp., from dioxan).

Sources & evidence

ORD record
ord-cb0ecebfa4314ec4abb96545e071d167
Source dataset
uspto-grants-1987_07
Patent number
US04678792

Reaction notes

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