HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylhydroxylamine → HCID 14224089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylhydroxylamine | HCID 69297 | — |
| Reactant | N,N'-o-phenylenedimaleimide | HCID 83156 | — |
| Product | HCID 14224089 | HCID 14224089 | 67.9% |
Reaction Steps
The procedure of Example 1 is repeated using 5.33 g (25 mmole) of N,N-dibenzylhydroxylamine and 3.35 g (12.5 mmole) of N,N'-ortho-phenylenedimaleimide. The residue is purified by preparative HPLC (Silica gel: 7:3 heptane:ethyl acetate eluent) to give 5.9 g (34%) of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04678826 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-357d48fb6a3f4c5ca4bdbedddc3590bd |
| Source note | uspto-grants-1987_07 |