Ethanol → Ethyl N-phenylcarbamate

HRID 2118575Notes

Reaction equation

HRID 2118575 reaction equation
C1(N[C:8]([NH:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:9])C=CC=CC=1.[CH2:17]([OH:19])[CH3:18]>>[CH3:18][CH2:17][O:19][C:8]([NH:10][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)=[O:9]

Participants

3

Reactant 2

HCID 702EthanolHCID 7595Carbanilide

Product 1

HCID 7591Ethyl N-phenylcarbamateYield 93%

Procedure

Following the same procedures as in Example 8, a total amount of N,N'-diphenyl urea crystal was reacted with 50.00 g of ethyl alcohol. After the reaction, the reaction mixture was analyzed to obtain a 93% yield for N-phenylethyl carbamate and a 95% yield for aniline.

Workup

  1. customAfter the reaction

Sources & evidence

ORD record
ord-774db3004bff45c9b3a26f491848b86e
Source dataset
uspto-grants-1987_07
Patent number
US04678856

Reaction notes

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