HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethoxycarbonylaminoindan-2-carboxylic Acid → HCID 88121557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethoxycarbonylaminoindan-2-carboxylic Acid | HCID 14012618 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 88121557 | HCID 88121557 | 59% |
Reaction Steps
The resultant compound of Example 4 (500 mg, 2.00 mmol) was dissolved in thionyl chloride (3 ml). Evaporation after 17 hours provided a solid which was recrystallized from ethyl acetate/hexane to give 239 mg (59%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680284 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-6a98af2d20c04fdf8983bb17fcd42712 |
| Source note | uspto-grants-1987_07 |