Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4,7-Dichloroquinoline | HCID 6866 | — |
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20192899 | HCID 20192899 | — |
Reaction Steps
17.1 Grams of hexane-1,6-diamine and 4.3 g of 4,7-dichloroquinoline were mixed together and heated to 150° C. for four hours. The reaction was cooled and water and methylene chloride were then added. The organic phase was washed, dried with anhydrous magnesium sulfate and evaporated thereby affording 1-amino-6-(7-chloro-4-quinolinyl)hexane having a melting point of 133°-134°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04680300 |
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| Source dataset | uspto-grants-1987_07 |
|---|
| ORD ID | ord-2dcff2bd2b0a4ac9b39f3a55291eb36e |
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| Source note | uspto-grants-1987_07 |
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