HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20192907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-[(6-Chlorohexyl)oxy]-1,1′-biphenyl | HCID 20192895 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20192907 | HCID 20192907 | — |
Reaction Steps
A solution of 1-(2-biphenyloxy)-6-chlorohexane 8.0 g) and potassium phtalimide (5.6 g) in dimethylformamide (100) ml) was heated at reflux temperature for 3 hours. The solution was cooled and poured into water, and the product was extracted out with ethyl acetate. The extract was dried and evaporated to afford N-[6-(biphenyloxy)hexyl]phthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680300 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-39d4ad115f194e5482c6d01a12fca396 |
| Source note | uspto-grants-1987_07 |