HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 13633449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Azacyclonol | HCID 15723 | — |
| Reactant | 1-(2-Bromoethyl)-1,3-dihydro-2H-benzimidazol-2-one | HCID 13633448 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | HCID 13633449 | HCID 13633449 | — |
Reaction Steps
A mixture of 2.7 g (0.01 mole) of alpha,alpha-diphenyl-4-piperidinemethanol, 2.4 g (0.01 mole) of 1-(1-bromo-2-ethyl)-2-benzimidazolone, 1.2 g of sodium carbonate (Na2CO3), and a crystal of sodium iodide in 75 ml of methyl isobutyl ketone is heated at reflux temperature for 18 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680296 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-0223bb8ed0f14cafbd55fe9435efec97 |
| Source note | uspto-grants-1987_07 |