HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecylamine → HCID 13361730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecylamine | HCID 13583 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13361730 | HCID 13361730 | — |
Reaction Steps
18 g of glucose are stirred in 50 ml of ethanol at 70° C., then 18.5 g of dodecylamine are added, heating is continued until a clear solution is obtained, and this is allowed to cool to room temperature and, after 20 hours, the crystals which have separated out are filtered off with suction. They are washed with ethanol and ether and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680287 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-0930781d79974684be016b8bbf67121b |
| Source note | uspto-grants-1987_07 |