Dodecylamine → HCID 13361730, compound

HRID 2118699Notes

Reaction equation

HRID 2118699 reaction equation
O=[CH:2][C@@H:3]([C@H:5]([C@@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:13]([NH2:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>C(O)C>[CH2:13]([NH:25][C@@H:2]1[O:10][C@H:9]([CH2:11][OH:12])[C@@H:7]([OH:8])[C@H:5]([OH:6])[C@H:3]1[OH:4])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

4

Reactant 2

HCID 13583DodecylamineHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal

Product 1

HCID 13361730HCID 13361730, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

18 g of glucose are stirred in 50 ml of ethanol at 70° C., then 18.5 g of dodecylamine are added, heating is continued until a clear solution is obtained, and this is allowed to cool to room temperature and, after 20 hours, the crystals which have separated out are filtered off with suction. They are washed with ethanol and ether and dried in vacuo.

Workup

  1. temperatureheating
  2. customis obtained
  3. customthe crystals which have separated out
  4. filtrationare filtered off with suction
  5. washThey are washed with ethanol and ether
  6. customdried in vacuo

Sources & evidence

ORD record
ord-0930781d79974684be016b8bbf67121b
Source dataset
uspto-grants-1987_07
Patent number
US04680287

Reaction notes

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