HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octadecylamine → HCID 13361751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | (2R,3S,4S,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 3037556 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 13361751 | HCID 13361751 | — |
Reaction Steps
60 g of D-galactose are suspended in 330 ml of isopropanol and 170 ml of water, and the mixture is heated to 50°. After addition of 90 g of stearylamine, the mixture is stirred until all the amine has gone into solution. On cooling, the glycosylamine crystallizes out. The solid is filtered off with suction, washed consecutively with ethanol and with ether, and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680287 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-280102638a4649a485330602bae45bc0 |
| Source note | uspto-grants-1987_07 |