HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20192951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Tert-butyl-5-chloro-6-nitrobenzothiazole | HCID 19794202 | — |
| Solvent | Morpholine | HCID 8083 | — |
| Product | HCID 20192951 | HCID 20192951 | — |
Reaction Steps
A solution of 170 g of 2-tert-butyl-5-chloro-6-nitrobenzothiazole described in Example 5, in 200 ml of morpholine is refluxed for 6.5 hours, cooled and poured into water. The solid is filtered, washed with water and cold alcohol to give 2-tert-butyl-5-[morpholin-4-yl]-6-nitrobenzothiazole melting at 119°-121°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680301 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-7f49cfba27f64dbfb4625e46239e956b |
| Source note | uspto-grants-1987_07 |