Methyl Methacrylate → HCID 21864285, compound

HRID 2118768Notes

Reaction equation

HRID 2118768 reaction equation
[C:1]([O:6]C)(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O:12]CCCC)(=[O:11])[CH:9]=[CH2:10]>O.O.O.O.O.O.[Co](Cl)Cl.CCC(C)=O>[C:1]([O-:6])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O-:12])(=[O:11])[CH:9]=[CH2:10]

Participants

5

Reactant 2

HCID 6658Methyl MethacrylateHCID 8846Butyl Acrylate

Product 1

HCID 21864285HCID 21864285, compound

Reagents, catalysts & solvents 2

HCID 517166Dichlorocobalt hexahydrateCatalystHCID 6569Methyl Ethyl KetoneSolvent

Procedure

Equal amounts of (5 gms. each) of methyl methacrylate and butyl acrylate were used, 1% (by weight) of AIBN (azoisobutyronitrile) were dissolved in 2.5 ml. MEK was added to the test tube and blanketed by nitrogen flushing. 480 ppm of cobalt chloride hexahydrate (CoCl2.6H2O) containing catalyst solution 1-A were added to the test tube and further flushed by N2 for 30 minutes.

Workup

  1. additionwere added to the test tube
  2. customfurther flushed by N2 for 30 minutes

Sources & evidence

ORD record
ord-8a10ba60467b4d44b2fda7218464b263
Source dataset
uspto-grants-1987_07
Patent number
US04680354

Reaction notes

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