HRID2118810

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10112

Calcium carbonate

CCaO3

HCID79081

3-Methylpiperidine

C6H13N

结构：O=C(c1ccc(Cl)cc1)c1cc([N+](=O)[O-])ccc1Cl

HCID875720

未命名化合物

PRODUCTS

生成物

结构：CC1CCCN(c2ccc([N+](=O)[O-])cc2C(=O)c2ccc(Cl)cc2)C1

HCID15072459

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Proceeding as in example 2, with 0.035 mole (10.4 g) of 2,4'-dichloro-5-nitro-benzophenone, 0.07 mole (7 cm3) of 3-methylpiperidine and 0.035 mole (5 g) of calcium carbonate mixed in ethanol, 12 g (Yield : 96%) of the expected product are obtained. M.P. 112° C.