HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Carbonate → [2-(3-Methyl-1-piperidinyl)-5-nitrophenyl]-(4-chlorophenyl)-methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | 3-Methylpiperidine | HCID 79081 | — |
| Reactant | (2-Chloro-5-nitro-phenyl)-(4-chloro-phenyl)-methanone | HCID 875720 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | [2-(3-Methyl-1-piperidinyl)-5-nitrophenyl]-(4-chlorophenyl)-methanone | HCID 15072459 | — |
Reaction Steps
Proceeding as in example 2, with 0.035 mole (10.4 g) of 2,4'-dichloro-5-nitro-benzophenone, 0.07 mole (7 cm3) of 3-methylpiperidine and 0.035 mole (5 g) of calcium carbonate mixed in ethanol, 12 g (Yield : 96%) of the expected product are obtained. M.P. 112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680402 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-fd36d45ac18d465a81bd04f1df6482eb |
| Source note | uspto-grants-1987_07 |