HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Carbonate → HCID 15072431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | 4-Methylpiperidine | HCID 69381 | — |
| Reactant | HCID 884746 | HCID 884746 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15072431 | HCID 15072431 | 95% |
Reaction Steps
Proceeding as in example 2, with 0.045 mole (13 g) of 2-chloro-4'-methyl-5-nitro-benzophenone, 0.1 mole (11.3 cm3) of 4-methyl piperidine and 0.045 mole (6.2 g) of calcium carbonate mixed in ethanol, 14 g (Yield: 95%) of the expected product are obtained. M.P. 86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680402 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-4fa9e9a6862f4bbf8d2d4efa13768816 |
| Source note | uspto-grants-1987_07 |