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HRID2118813

反应详情

EQUATION

反应方程式

HRID 2118813 的结构方程式

REACTANTS

反应物

3
结构：CC1CCCCN1
HCID7974

2-Methylpiperidine

C6H13N

结构：O=C([O-])[O-].[Ca+2]
HCID10112

Calcium carbonate

CCaO3

结构：O=C(c1ccc(Cl)cc1)c1cc([N+](=O)[O-])ccc1Cl
HCID875720

未命名化合物

PRODUCTS

生成物

1
结构：CC1CCCCN1c1ccc([N+](=O)[O-])cc1C(=O)c1ccc(Cl)cc1
HCID15072474

未命名化合物

收率 40.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Proceeding as indicated in example 2, from 0.035 mole (10.4 g) of 2,4'-dichloro-5-nitro-benzophenone, 0.07 mole (7 cm3) of 2-methylpiperidine and 0.035 mole (5 g) of calcium carbonate in ethanol, 5.1 g (Yield: 40%) of the expected product are obtained after recrystallization in ethanol. M.P. 142° C.