HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Carbonate → HCID 15072434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | 4-Methylpiperidine | HCID 69381 | — |
| Reactant | (2-Chloro-5-nitrophenyl)(4-methoxyphenyl)methanone | HCID 885157 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15072434 | HCID 15072434 | 54.2% |
Reaction Steps
Proceeding as indicated in example 2, with 0.0635 mole (18.5 g) of 2-chloro-4'-methoxy-5-nitro-benzophenone, 0.076 mole (10.5 g) of calcium carbonate and 0.127 mole (12.57 g) of 4-methyl piperidine in 50 cm3 of ethanol, 12.2 g (Yield: 53%) of the expected product are obtained. M.P. 119° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680402 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-5d65e4fba00d464db268db625dbd84c8 |
| Source note | uspto-grants-1987_07 |