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HRID2118814

反应详情

EQUATION

反应方程式

HRID 2118814 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Ca+2]
HCID10112

Calcium carbonate

CCaO3

结构：CC1CCNCC1
HCID69381

Piperidine, 4-methyl-

C6H13N

结构：COc1ccc(C(=O)c2cc([N+](=O)[O-])ccc2Cl)cc1
HCID885157

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C(=O)c2cc([N+](=O)[O-])ccc2N2CCC(C)CC2)cc1
HCID15072434

未命名化合物

收率 54.2%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Proceeding as indicated in example 2, with 0.0635 mole (18.5 g) of 2-chloro-4'-methoxy-5-nitro-benzophenone, 0.076 mole (10.5 g) of calcium carbonate and 0.127 mole (12.57 g) of 4-methyl piperidine in 50 cm3 of ethanol, 12.2 g (Yield: 53%) of the expected product are obtained. M.P. 119° C.