HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Carbonate → HCID 15072476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | 4-Methylpiperidine | HCID 69381 | — |
| Reactant | (2-Chloro-5-nitrophenyl)(2,4-dichlorophenyl)methanone | HCID 15072475 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15072476 | HCID 15072476 | 75% |
Reaction Steps
Proceeding as indicated in example 2, with 0.053 mole (17.5 g) of 2,2',4'-trichloro-5-nitro-benzophenone, 0.088 mole (8.8 g) of 4-methylpiperidine and 0.0712 mole (9.8 g) of calcium carbonate in 50 cm3 of ethanol, 15.5 g (Yield: 75%) of the expected product are obtained after re-crystallization in a mixture of isopropyl ether and toluene (70 v./30 v.) M.P.: 103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680402 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-a01c0a66fa2c49968753c2718491e781 |
| Source note | uspto-grants-1987_07 |