Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20191699 | HCID 20191699 | — |
| Product | HCID 13851472 | HCID 13851472 | — |
Reaction Steps
To a suspension of sodium hydride (3.20 g, 60% dispersion in oil, washed twice with hexane) in 20 ml dimethylformamide/benzene (20:80) was added a solution of [1-(2-fluorobenzyl)-5-methylpyrrol-2-yl][(1-methyl)piperidin-4-yl]methanol (15.45 g, 0.088 mole) in 80 ml of the same solvent. This was heated at 70° C. for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04681879 |
|---|
| Source dataset | uspto-grants-1987_07 |
|---|
| ORD ID | ord-aaad76e4d7d84c68a812a896ebdf46d8 |
|---|
| Source note | uspto-grants-1987_07 |
|---|
