HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13921373, compound → 4-Pyridinylacetone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13921373 | HCID 13921373 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Pyridinylacetone | HCID 80552 | 98.3% |
Reaction Steps
To 20 g of 1-acetyl-4(acetylmethylidene)-1,4-dihydropyridine was added 30 ml ethanol and the mixture refluxed 4 to 8 hours. Upon removal of solvent, 15 g of 1-(4-pyridinyl)-2-propanone was obtained as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04681944 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-d589c2fb3b03486bb70d18bf60ac9913 |
| Source note | uspto-grants-1987_07 |