HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 14010404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2'-Hydroxybenzophenone | HCID 8348 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14010404 | HCID 14010404 | — |
Reaction Steps
1 g. (0.005 mole) of O-hydroxybenzophenone was warmed in 25 mls of dry pyridine containing 1 g (0.01 mole) of pivaloyl chloride for 3 hrs. at 50° C. Poured into H2O containing 2 g of Na2CO3 and extracted with EtOAc+Et2O and washed with H2O. After drying over Na2SO4 and filtration, the product was isolated by evaporation of the solvent. Oily material. 1.2 g. (85%) yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04683241 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-676a8f024a8d4ddfa68a1c26437c4637 |
| Source note | uspto-grants-1987_07 |