HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 14010405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 2,2'-Dihydroxybenzophenone | HCID 70038 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 14010405 | HCID 14010405 | — |
Reaction Steps
2 g (0.01 mole) of 2,2'-dihydroxybenzophenone was dissolved in 30 mls of dry pyridine and 3 g (0.03 mole) of pivaloyl chloride added and contents warmed for 3 hrs. at 50° C. Solvent was removed by rotary evaporator and H2O added and crystals filtered. Recrystallized from ethanol, 3.2 g (83%) yield, M.P.~106°-108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04683241 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-706e9094ad9e4936a5620f3684d5f871 |
| Source note | uspto-grants-1987_07 |