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HRID2119189

反应详情

EQUATION

反应方程式

HRID 2119189 的结构方程式

REACTANTS

反应物

2
结构：C=C(C)C(=O)Cl
HCID13528

Methacryloyl chloride

C4H5ClO

结构：O=C(c1ccccc1)c1ccc(O)cc1
HCID14347

4-Hydroxybenzophenone

C13H10O2

PRODUCTS

生成物

1
结构：C=C(C)C(=O)Oc1ccc(C(=O)c2ccccc2)cc1
HCID11230895

4-Benzoylphenyl methacrylate

C17H14O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

Prepared from 6.0 g of 4-hydroxybenzophenone and 4.4 ml of methacryloyl chloride in 70 ml of pyridine. Recrystallized from ethyl acetate-ethanol-water; M.P.~69.5°-70.5° C.

WORKUP

后处理

  1. customRecrystallized from ethyl acetate-ethanol-water