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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2119294Generated: November 1, 2026

HCID 69902277, compound → HCID 12971812, compound

https://huagongshe.com/reaction/2119294

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69902277HCID 69902277—
ReactantHCID 86585951HCID 86585951—
SolventPyridineHCID 1049—
ProductHCID 12971812HCID 12971812—

Reaction Conditions

Temperature60 °C

Reaction Steps

30 mmol of (5R)-4,5,6,7-tetrahydrofuro[2,3-c]pyridine-5-carboxylic acid tert-butyl ester hydrochloride are placed in 150 ml of pyridine. 30 mmol of 2-(4-pyridyl)-1-benzofuran-5-sulphonyl chloride described in Preparation C are then added at room temperature and the whole is heated at 60° C. overnight.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06686348B2
Source datasetuspto-grants-2004_02
ORD IDord-7138e84762214165b2aab2371546f4c6
Source noteuspto-grants-2004_02