HRID2119327

反应详情

EQUATION

反应方程式

HRID 2119327 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of N-benzyl-N-methyl-5-(4-morpholinylmethyl)-2-nitroaniline (3.3 g, 9.7 mmol) and 10% palladium charcoal (0.25 g) in ethyl acetate (100 mL) is hydrogenated (50 psi initial hydrogen pressure) until HPLC shows that reaction is complete (40 min). The solvent is evaporated to give 3.1 g of the title compound as an oil.

WORKUP

后处理

  1. customshows that reaction
  2. custom(40 min)
  3. customThe solvent is evaporated