HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 69891115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 23441016 | HCID 23441016 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69891115 | HCID 69891115 | — |
Reaction Steps
Trifluoroacetic acid (4.75 mL) was added to a solution of 1-[3-hydroxy-3-(3-hydroxyphenyl)-3-phenylpropyl]homopiperazine (Compound No. 295, 60 mg, 0.184 mmol) in CH2Cl2 (0.25 mL). The reaction mixture was stirred at room temperature for 2.5 h. The trifluoroacetic acid was evaporated to afford 1-[3-(3-hydroxyphenyl)-3-phenyl-2-propenyl]homopiperazine as a colorless oil used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686353B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-78aa8182be53469796f47ee7c1e73ca5 |
| Source note | uspto-grants-2004_02 |