Dimethylformamide dimethyl acetal → HCID 73686215, compound

HRID 2119584Notes

Reaction equation

HRID 2119584 reaction equation
[C:1]([O:5][C:6](=[O:17])[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][NH:13][C:14]([NH2:16])=[S:15])([CH3:4])([CH3:3])[CH3:2].CO[CH:20](OC)[N:21]([CH3:23])[CH3:22]>>[C:1]([O:5][C:6](=[O:17])[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][NH:13][C:14]([N:16]=[CH:20][N:21]([CH3:23])[CH3:22])=[S:15])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 22254010HCID 22254010, compound

Product 1

HCID 73686215HCID 73686215, compoundYield 54%

Procedure

The title compound was synthesized from (5-Thioureido-pentyl)-carbamic acid tert-butyl ester and Dimethylformamide dimethyl acetal according to the procedure described for Example C in 54% yield.

Sources & evidence

ORD record
ord-2768f9cab1c340a5b3a739dfc1e38a9d
Source dataset
uspto-grants-2004_02
Patent number
US06686381B2

Reaction notes

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