HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23442618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 20616913 | HCID 20616913 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 23442618 | HCID 23442618 | 99% |
Reaction Steps
A solution of 170 mg (0.4 mmol) {5-[4-Methyl-5-(2-methyl-benzoyl)-thiazol-2-ylamino]-pentyl}-carbamic acid tert-butyl ester in 2 ml dioxane was treated with 1 ml 4N HCl in dioxane and allowed to react for 5 h at room temperature. The mixture was evaporated under reduced pressure to afford 143 mg (99%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686381B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-37758d9a98014eb6b23dc10e117b6d94 |
| Source note | uspto-grants-2004_02 |