HRID2119600

反应详情

EQUATION

反应方程式

HRID 2119600 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 170 mg (0.4 mmol) {5-[4-Methyl-5-(2-methyl-benzoyl)-thiazol-2-ylamino]-pentyl}-carbamic acid tert-butyl ester in 2 ml dioxane was treated with 1 ml 4N HCl in dioxane and allowed to react for 5 h at room temperature. The mixture was evaporated under reduced pressure to afford 143 mg (99%) of the title compound.

WORKUP

后处理

  1. customto react for 5 h at room temperature
  2. customThe mixture was evaporated under reduced pressure