Dimethylformamide dimethyl acetal → HCID 72522556, compound

HRID 2119602Notes

Reaction equation

HRID 2119602 reaction equation
[C:1]([O:5][C:6](=[O:14])[NH:7][CH2:8][CH2:9][NH:10][C:11]([NH2:13])=[S:12])([CH3:4])([CH3:3])[CH3:2].CO[CH:17](OC)[N:18]([CH3:20])[CH3:19]>>[C:1]([O:5][C:6](=[O:14])[NH:7][CH2:8][CH2:9][NH:10][C:11]([N:13]=[CH:17][N:18]([CH3:20])[CH3:19])=[S:12])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 22726781HCID 22726781, compound

Product 1

HCID 72522556HCID 72522556, compoundYield 51%

Procedure

The title compound was synthesised from (2-Thioureido-ethyl)-carbamic acid tert-butyl ester and Dimethylformamide dimethyl acetal according to the procedure described for Example C in 51% yield. MS (m/e): 275.4 (MH+, 100%).

Sources & evidence

ORD record
ord-93c4333a333a4c82bf55aa5bcf2af307
Source dataset
uspto-grants-2004_02
Patent number
US06686381B2

Reaction notes

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