Dimethylformamide dimethyl acetal → HCID 72522555, compound

HRID 2119604Notes

Reaction equation

HRID 2119604 reaction equation
[C:1]([O:5][C:6](=[O:16])[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][NH:12][C:13]([NH2:15])=[S:14])([CH3:4])([CH3:3])[CH3:2].CO[CH:19](OC)[N:20]([CH3:22])[CH3:21]>>[C:1]([O:5][C:6](=[O:16])[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][NH:12][C:13]([N:15]=[CH:19][N:20]([CH3:22])[CH3:21])=[S:14])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 22253970HCID 22253970, compound

Product 1

HCID 72522555HCID 72522555, compoundYield 76%

Procedure

The title compound was synthesised from (4-Thioureido-butyl)-carbamic acid tert-butyl ester and Dimethylformamide dimethyl acetal according to the procedure described for Example C in 76% yield. MS (m/e): 303.3 (MH+, 100%).

Sources & evidence

ORD record
ord-05a47c6b6c5842c5bc6dbb446918fbed
Source dataset
uspto-grants-2004_02
Patent number
US06686381B2

Reaction notes

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