HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-2'-methylacetophenone → HCID 20616910, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-2'-methylacetophenone | HCID 12430676 | — |
| Reactant | HCID 72522555 | HCID 72522555 | — |
| Product | HCID 20616910 | HCID 20616910 | 69% |
Reaction Steps
The title compound was synthesised from [4-(3-Dimethylaminomethylene-thioureido)-butyl]-carbamic acid tert-butyl ester and 2-methyl phenacylbromide (Literature: WO9907666) according to the procedure described for Example 25 in 69% yield. MS (m/e): 390.2 (MH+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686381B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ffcc58dd248442e29aa86aa6f7eeb431 |
| Source note | uspto-grants-2004_02 |